Quantitative analysis of curing mechanisms of epoxy resin by mid- and near-fourier transform infra red spectroscopy

Sagar T. Cholake; Mykanth R. Mada; R. K. Singh Raman; Yu Bai; X. L. Zhao; Sami Rizkalla; Sri Bandyopadhyay

doi:10.14429/dsj.64.7326

Quantitative analysis of curing mechanisms of epoxy resin by mid- and near-fourier transform infra red spectroscopy

Sagar T. Cholake, Mykanth R. Mada, R. K. Singh Raman, Yu Bai, X. L. Zhao, Sami Rizkalla, Sri Bandyopadhyay

Research output: Journal article publication › Journal article › Academic research › peer-review

88 Citations (Scopus)

Abstract

This article informs the essence of major work done by a number of researchers on the analysis of two-step curing mechanism of diglycidyl ether of bisphenol A (DGEBA) epoxy resin in presence of amine curing agents using near- and mid-IR technology. Various peaks used as a marker for resin formation are discussed and their implementation is comprehensively studied. In addition to this, a wide range of information about the importance of reference peaks in both near-IR (NIR) and mid-IR (MIR) regions are congregated and their accuracy is audited. Also discrepancies observed by researchers in epoxy conversion (α) in NIR and MIR regions are reviewed to highlight the comparative advantages of both regions, one over the other.

Original language	English
Pages (from-to)	314-321
Number of pages	8
Journal	Defence Science Journal
Volume	64
Issue number	3
DOIs	https://doi.org/10.14429/dsj.64.7326
Publication status	Published - May 2014
Externally published	Yes

Keywords

Amines
Curing
Epoxy resin
FTIR

ASJC Scopus subject areas

General Chemical Engineering
Biomedical Engineering
Mechanical Engineering
General Physics and Astronomy
Computer Science Applications
Electrical and Electronic Engineering

More information

10.14429/dsj.64.7326

Cite this

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title = "Quantitative analysis of curing mechanisms of epoxy resin by mid- and near-fourier transform infra red spectroscopy",

abstract = "This article informs the essence of major work done by a number of researchers on the analysis of two-step curing mechanism of diglycidyl ether of bisphenol A (DGEBA) epoxy resin in presence of amine curing agents using near- and mid-IR technology. Various peaks used as a marker for resin formation are discussed and their implementation is comprehensively studied. In addition to this, a wide range of information about the importance of reference peaks in both near-IR (NIR) and mid-IR (MIR) regions are congregated and their accuracy is audited. Also discrepancies observed by researchers in epoxy conversion (α) in NIR and MIR regions are reviewed to highlight the comparative advantages of both regions, one over the other.",

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AU - Cholake, Sagar T.

AU - Mada, Mykanth R.

AU - Singh Raman, R. K.

AU - Bai, Yu

AU - Zhao, X. L.

AU - Rizkalla, Sami

AU - Bandyopadhyay, Sri

PY - 2014/5

Y1 - 2014/5

N2 - This article informs the essence of major work done by a number of researchers on the analysis of two-step curing mechanism of diglycidyl ether of bisphenol A (DGEBA) epoxy resin in presence of amine curing agents using near- and mid-IR technology. Various peaks used as a marker for resin formation are discussed and their implementation is comprehensively studied. In addition to this, a wide range of information about the importance of reference peaks in both near-IR (NIR) and mid-IR (MIR) regions are congregated and their accuracy is audited. Also discrepancies observed by researchers in epoxy conversion (α) in NIR and MIR regions are reviewed to highlight the comparative advantages of both regions, one over the other.

AB - This article informs the essence of major work done by a number of researchers on the analysis of two-step curing mechanism of diglycidyl ether of bisphenol A (DGEBA) epoxy resin in presence of amine curing agents using near- and mid-IR technology. Various peaks used as a marker for resin formation are discussed and their implementation is comprehensively studied. In addition to this, a wide range of information about the importance of reference peaks in both near-IR (NIR) and mid-IR (MIR) regions are congregated and their accuracy is audited. Also discrepancies observed by researchers in epoxy conversion (α) in NIR and MIR regions are reviewed to highlight the comparative advantages of both regions, one over the other.

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KW - Curing

KW - Epoxy resin

KW - FTIR

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DO - 10.14429/dsj.64.7326

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Quantitative analysis of curing mechanisms of epoxy resin by mid- and near-fourier transform infra red spectroscopy

Abstract

Keywords

ASJC Scopus subject areas

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