N,N′-(Ethane-1,2-diyl)bis(methanesulfonamide)

Wesley Ting Kwok Chan; Ka Yan Karen Kung; Man Kin Wong

doi:10.1107/S1600536814000622

N,N′-(Ethane-1,2-diyl)bis(methanesulfonamide)

Wesley Ting Kwok Chan, Ka Yan Karen Kung, Man Kin Wong

Research output: Journal article publication › Journal article › Academic research › peer-review

Abstract

The molecular structure of the title compound, C4H12N2O4S2, has crystallographic inversion symmetry. The central N - C - C - N moiety was refined as disordered over two sets of sites with an approximate occupancy ratio of 3:1 [0.742(15):0.258(15). In the crystal, N - HO hydrogen bonds link adjacent molecules into a thick sheet structure parallel to the b-axis direction. 2014.

Original language	English
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	70
Issue number	2
DOIs	https://doi.org/10.1107/S1600536814000622
Publication status	Published - 1 Feb 2014

Keywords

data-to-parameter ratio = 14.7
disorder in main residue
mean σ(S-C) = 0.002 Å
R factor = 0.032
single-crystal X-ray study
T = 296 K
wR factor = 0.099

ASJC Scopus subject areas

Condensed Matter Physics
General Materials Science
General Chemistry

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10.1107/S1600536814000622

http://10.1107/S1600536814000622

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title = "N,N′-(Ethane-1,2-diyl)bis(methanesulfonamide)",

abstract = "The molecular structure of the title compound, C4H12N2O4S2, has crystallographic inversion symmetry. The central N - C - C - N moiety was refined as disordered over two sets of sites with an approximate occupancy ratio of 3:1 [0.742(15):0.258(15). In the crystal, N - HO hydrogen bonds link adjacent molecules into a thick sheet structure parallel to the b-axis direction. 2014.",

keywords = "data-to-parameter ratio = 14.7, disorder in main residue, mean σ(S-C) = 0.002 {\AA}, R factor = 0.032, single-crystal X-ray study, T = 296 K, wR factor = 0.099",

author = "Chan, {Wesley Ting Kwok} and Kung, {Ka Yan Karen} and Wong, {Man Kin}",

year = "2014",

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T1 - N,N′-(Ethane-1,2-diyl)bis(methanesulfonamide)

AU - Chan, Wesley Ting Kwok

AU - Kung, Ka Yan Karen

AU - Wong, Man Kin

PY - 2014/2/1

Y1 - 2014/2/1

N2 - The molecular structure of the title compound, C4H12N2O4S2, has crystallographic inversion symmetry. The central N - C - C - N moiety was refined as disordered over two sets of sites with an approximate occupancy ratio of 3:1 [0.742(15):0.258(15). In the crystal, N - HO hydrogen bonds link adjacent molecules into a thick sheet structure parallel to the b-axis direction. 2014.

AB - The molecular structure of the title compound, C4H12N2O4S2, has crystallographic inversion symmetry. The central N - C - C - N moiety was refined as disordered over two sets of sites with an approximate occupancy ratio of 3:1 [0.742(15):0.258(15). In the crystal, N - HO hydrogen bonds link adjacent molecules into a thick sheet structure parallel to the b-axis direction. 2014.

KW - data-to-parameter ratio = 14.7

KW - disorder in main residue

KW - mean σ(S-C) = 0.002 Å

KW - R factor = 0.032

KW - single-crystal X-ray study

KW - T = 296 K

KW - wR factor = 0.099

UR - http://www.scopus.com/inward/record.url?scp=84893652396&partnerID=8YFLogxK

U2 - 10.1107/S1600536814000622

DO - 10.1107/S1600536814000622

M3 - Journal article

SN - 1600-5368

VL - 70

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 2

ER -

N,N′-(Ethane-1,2-diyl)bis(methanesulfonamide)

Abstract

Keywords

ASJC Scopus subject areas

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