Facile solution synthesis and characterization of CaCO3microspheres with urchin-shaped structure

Wenshuang Zhang; Xinyong Li; Zhenping Qu; Qidong Zhao; Guohua Chen

doi:10.1016/j.matlet.2009.10.009

Facile solution synthesis and characterization of CaCO₃microspheres with urchin-shaped structure

Wenshuang Zhang, Xinyong Li, Zhenping Qu, Qidong Zhao, Guohua Chen

Research output: Journal article publication › Journal article › Academic research › peer-review

23 Citations (Scopus)

Abstract

Urchin-shaped CaCO3microspheres were successfully synthesized by a facile low-temperature solution-phase method. The product was characterized with X-ray diffraction (XRD), Raman spectra and high resolution transmission electron microscopy (HRTEM). The characterization results revealed that the structure of the urchin-shaped CaCO3was grown along the (104) crystal plane with a calcite structure. Furthermore, the valence states and the surface chemical compositions of CaCO3were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare urchin-shaped CaCO3microspheres in large scale, which broads their practical applications.

Original language	English
Pages (from-to)	71-73
Number of pages	3
Journal	Materials Letters
Volume	64
Issue number	1
DOIs	https://doi.org/10.1016/j.matlet.2009.10.009
Publication status	Published - 15 Jan 2010
Externally published	Yes

Keywords

Calcium carbonate
Characterization methods
Microstructure
Three-dimensional
Urchin-shaped

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

More information

10.1016/j.matlet.2009.10.009

Cite this

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abstract = "Urchin-shaped CaCO3microspheres were successfully synthesized by a facile low-temperature solution-phase method. The product was characterized with X-ray diffraction (XRD), Raman spectra and high resolution transmission electron microscopy (HRTEM). The characterization results revealed that the structure of the urchin-shaped CaCO3was grown along the (104) crystal plane with a calcite structure. Furthermore, the valence states and the surface chemical compositions of CaCO3were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare urchin-shaped CaCO3microspheres in large scale, which broads their practical applications.",

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AU - Zhang, Wenshuang

AU - Li, Xinyong

AU - Qu, Zhenping

AU - Zhao, Qidong

AU - Chen, Guohua

PY - 2010/1/15

Y1 - 2010/1/15

N2 - Urchin-shaped CaCO3microspheres were successfully synthesized by a facile low-temperature solution-phase method. The product was characterized with X-ray diffraction (XRD), Raman spectra and high resolution transmission electron microscopy (HRTEM). The characterization results revealed that the structure of the urchin-shaped CaCO3was grown along the (104) crystal plane with a calcite structure. Furthermore, the valence states and the surface chemical compositions of CaCO3were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare urchin-shaped CaCO3microspheres in large scale, which broads their practical applications.

AB - Urchin-shaped CaCO3microspheres were successfully synthesized by a facile low-temperature solution-phase method. The product was characterized with X-ray diffraction (XRD), Raman spectra and high resolution transmission electron microscopy (HRTEM). The characterization results revealed that the structure of the urchin-shaped CaCO3was grown along the (104) crystal plane with a calcite structure. Furthermore, the valence states and the surface chemical compositions of CaCO3were further identified by X-ray photoelectron spectroscopy (XPS). This study provides a simple method to prepare urchin-shaped CaCO3microspheres in large scale, which broads their practical applications.

KW - Calcium carbonate

KW - Characterization methods

KW - Microstructure

KW - Three-dimensional

KW - Urchin-shaped

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