Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate

Sohail Saeed; Naghmana Rashid; Wing Tak Wong

doi:10.1107/S1600536810011116

Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate

Sohail Saeed, Naghmana Rashid, Wing Tak Wong

Research output: Journal article publication › Journal article › Academic research › peer-review

4 Citations (Scopus)

Abstract

In the title compound, C17H15N3O 5S, the nitro and thio-ureido groups are twisted by 7.2 (7) and 21.4 (2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0 (1) and 18.0 (2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N - H⋯O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N - H⋯O hydrogen bonds connect the mol-ecules into chains running along the a axis.

Original language	English
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	66
Issue number	4
DOIs	https://doi.org/10.1107/S1600536810011116
Publication status	Published - 28 Apr 2010

ASJC Scopus subject areas

Condensed Matter Physics
General Materials Science
General Chemistry

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10.1107/S1600536810011116

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title = "Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate",

abstract = "In the title compound, C17H15N3O 5S, the nitro and thio-ureido groups are twisted by 7.2 (7) and 21.4 (2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0 (1) and 18.0 (2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N - H⋯O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N - H⋯O hydrogen bonds connect the mol-ecules into chains running along the a axis.",

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T1 - Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate

AU - Saeed, Sohail

AU - Rashid, Naghmana

AU - Wong, Wing Tak

PY - 2010/4/28

Y1 - 2010/4/28

N2 - In the title compound, C17H15N3O 5S, the nitro and thio-ureido groups are twisted by 7.2 (7) and 21.4 (2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0 (1) and 18.0 (2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N - H⋯O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N - H⋯O hydrogen bonds connect the mol-ecules into chains running along the a axis.

AB - In the title compound, C17H15N3O 5S, the nitro and thio-ureido groups are twisted by 7.2 (7) and 21.4 (2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0 (1) and 18.0 (2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N - H⋯O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N - H⋯O hydrogen bonds connect the mol-ecules into chains running along the a axis.

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U2 - 10.1107/S1600536810011116

DO - 10.1107/S1600536810011116

M3 - Journal article

SN - 1600-5368

VL - 66

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 4

ER -

Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate

Abstract

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