A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism

Sohail Saeed; Wing Tak Wong

doi:10.1002/jhet.820

A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism

Sohail Saeed
, Wing Tak Wong

Research output: Journal article publication › Journal article › Academic research › peer-review

11 Citations (Scopus)

Abstract

A series of variously substituted 1,3-thiazole heterocyclic compounds (3a-3d) were prepared by base-catalyzed S-cyclization of corresponding 2,4-dichloro-N-{[(4-substitutedphenyl)amino]carbonothioyl}benzamide (2a-2d) with acetophenone in the presence of bromine. The structure of all compounds was established by IR, 1H-NMR, 13C-NMR, elemental analysis, and X-ray crystallographic analysis.

Original language	English
Pages (from-to)	580-584
Number of pages	5
Journal	Journal of Heterocyclic Chemistry
Volume	49
Issue number	3
DOIs	https://doi.org/10.1002/jhet.820
Publication status	Published - 1 May 2012
Externally published	Yes

ASJC Scopus subject areas

Organic Chemistry

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10.1002/jhet.820

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title = "A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism",

abstract = "A series of variously substituted 1,3-thiazole heterocyclic compounds (3a-3d) were prepared by base-catalyzed S-cyclization of corresponding 2,4-dichloro-N-\{[(4-substitutedphenyl)amino]carbonothioyl\}benzamide (2a-2d) with acetophenone in the presence of bromine. The structure of all compounds was established by IR, 1H-NMR, 13C-NMR, elemental analysis, and X-ray crystallographic analysis.",

author = "Sohail Saeed and Wong, \{Wing Tak\}",

year = "2012",

month = may,

day = "1",

doi = "10.1002/jhet.820",

language = "English",

volume = "49",

pages = "580--584",

journal = "Journal of Heterocyclic Chemistry",

issn = "0022-152X",

publisher = "John Wiley and Sons Inc.",

number = "3",

}

A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism. / Saeed, Sohail; Wong, Wing Tak.
In: Journal of Heterocyclic Chemistry, Vol. 49, No. 3, 01.05.2012, p. 580-584.

Research output: Journal article publication › Journal article › Academic research › peer-review

TY - JOUR

T1 - A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism

AU - Saeed, Sohail

AU - Wong, Wing Tak

PY - 2012/5/1

Y1 - 2012/5/1

N2 - A series of variously substituted 1,3-thiazole heterocyclic compounds (3a-3d) were prepared by base-catalyzed S-cyclization of corresponding 2,4-dichloro-N-{[(4-substitutedphenyl)amino]carbonothioyl}benzamide (2a-2d) with acetophenone in the presence of bromine. The structure of all compounds was established by IR, 1H-NMR, 13C-NMR, elemental analysis, and X-ray crystallographic analysis.

AB - A series of variously substituted 1,3-thiazole heterocyclic compounds (3a-3d) were prepared by base-catalyzed S-cyclization of corresponding 2,4-dichloro-N-{[(4-substitutedphenyl)amino]carbonothioyl}benzamide (2a-2d) with acetophenone in the presence of bromine. The structure of all compounds was established by IR, 1H-NMR, 13C-NMR, elemental analysis, and X-ray crystallographic analysis.

UR - https://www.scopus.com/pages/publications/84863850836

U2 - 10.1002/jhet.820

DO - 10.1002/jhet.820

M3 - Journal article

SN - 0022-152X

VL - 49

SP - 580

EP - 584

JO - Journal of Heterocyclic Chemistry

JF - Journal of Heterocyclic Chemistry

IS - 3

ER -

A simple, convenient, and efficient synthetic route for the preparation of (Z)-3,5-Dichloro-N-(3-(4-substitutedphenyl)-4-phenylthiazole-2(3H)-ylide) benzamide heterocyclic compounds from aroyl thiourea derivatives via s-cyclization mechanism

Abstract

ASJC Scopus subject areas

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